Cl₂Fe(OP(C₆H₅)2OCH₂)2CC₁₂H₈

Base Information

• Chemical Name: Cl₂Fe(OP(C₆H₅)2OCH₂)2CC₁₂H₈
• CAS No.: 1262230-35-2
• Molecular Formula: C₃₉H₃₂Cl₂FeO₄P₂
• Molecular Weight: 753.381
• Mol file: 1262230-35-2.mol

Synonyms:

Chemical Property of Cl₂Fe(OP(C₆H₅)2OCH₂)2CC₁₂H₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cl₂Fe(OP(C₆H₅)2OCH₂)2CC₁₂H₈

There total 1 articles about Cl₂Fe(OP(C₆H₅)2OCH₂)2CC₁₂H₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

9,9-bis((diphenylphosphinito)methyl)fluorene (1072903-94-6) + iron(II) chloride → Cl2Fe(OP(C6H5)2OCH2)2CC12H8 (1262230-35-2)

Guidance literature:

In tetrahydrofuran; Schlenk techniques used under N2, anhyd. FeCl2 added to soln. of 9,9-(Ph2POCH2)2-fluorene in THF, stirred at room temp. for 24 h; volatiles removed under vac., washed with diethyl ether, dissolved in CH2Cl2, pentane added; XRD;

DOI:10.1016/j.ica.2010.06.007

upstream raw materials:

9,9-bis((diphenylphosphinito)methyl)fluorene