methyl (+/-)-(methyl)-3-butenoate

Base Information

Chemical Name:methyl (+/-)-(methyl)-3-butenoate
CAS No.:123613-58-1
Molecular Formula:C₂₁H₂₃NO₄
Molecular Weight:353.418
Hs Code.:

methyl (+/-)-(<N-benzyl-N-(benzyloxycarbonyl)amino>methyl)-3-butenoate

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Suppliers and Price of methyl (+/-)-(methyl)-3-butenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (+/-)-(methyl)-3-butenoate

Chemical Property:

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Technology Process of methyl (+/-)-(methyl)-3-butenoate

There total 3 articles about methyl (+/-)-(methyl)-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 85636-50-6
1-(trimethylsiloxy)-1-methoxy-1,3-butadiene

: 123613-56-9
N-methoxymethyl benzylamine benzylcarbamate

: 123613-58-1
methyl (+/-)-(methyl)-3-butenoate

: 123613-57-0
methyl (E)--2-pentenoate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96112-5

Reference yield:

: 39896-97-4
benzyl-carbamic acid benzyl ester

: 123613-58-1
methyl (+/-)-(methyl)-3-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / 16 h / Ambient temperature

2: BF₃*OEt₂ / CH₂Cl₂ / 2 h / Ambient temperature

With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(00)99482-6

Reference yield:

: 119582-47-7
tert-butyl((1-methoxybuta-1,3-dien-1-yl)oxy)dimethylsilane

: 123613-56-9
N-methoxymethyl benzylamine benzylcarbamate

: 123613-58-1
methyl (+/-)-(methyl)-3-butenoate

: 123613-57-0
methyl (E)--2-pentenoate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 2h; Yield given. Yields of byproduct given; Ambient temperature;
DOI:10.1016/S0040-4039(00)99482-6