CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

Base Information

Chemical Name:CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄
CAS No.:1068599-48-3
Molecular Formula:C₂₁H₁₉BO₂S
Molecular Weight:346.258
Hs Code.:

CH<sub>3</sub>C<sub>6</sub>H<sub>4</sub>SCHCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>BO<sub>2</sub>C<sub>6</sub>H<sub>4</sub>

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Chemical Property of CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

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Technology Process of CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

There total 3 articles about CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 24182-83-0,92550-70-4,24182-84-1
(E)-styryl(p-tolyl)sulfane

: 274-07-7
benzo[1,3,2]dioxaborole

: 1068599-48-3
CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

: 156575-59-6
2-(2-phenylethyl)benzo-1,3,2-dioxaborole

Guidance literature:: Wilkinson's catalyst; In toluene; (N2), RhCl(PPh3)3 (5 mol%) in toluene added to (E)-2(p-toluenethio)styrene in toluene, treated dropwise with catecholborane (L:B=1.1.5), reactedat room temp. for 24 h; evapd.(vac.), dissolved (hexane), stored at -30°C, recrystd. twice (hexane);
DOI:10.1016/j.molcata.2007.05.026

Reference yield:

: 24182-83-0,92550-70-4,24182-84-1
(E)-styryl(p-tolyl)sulfane

: 274-07-7
benzo[1,3,2]dioxaborole

: 1068599-48-3
CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

: 156575-60-9
2-(1-phenyl-ethyl)-benzo[1,3,2]dioxaborole

Guidance literature:: With catalyst:Rh(acac)(coe)2/dppp; In benzene-d6; (N2), HBcat in C6D6 reacted with ligand at room temp. catalyzed by Rh(acac)(coe)2/dppp); not isolated, detected by NMR, chromy.;
DOI:10.1016/j.molcata.2007.05.026

Reference yield:

: 24182-83-0,92550-70-4,24182-84-1
(E)-styryl(p-tolyl)sulfane

: 274-07-7
benzo[1,3,2]dioxaborole

: 1068599-48-3
CH₃C₆H₄SCHCH₂C₆H₅BO₂C₆H₄

: 1068599-50-7
CH₃C₆H₄SCH₂CHBO₂C₆H₄C₆H₅

: 156575-60-9
2-(1-phenyl-ethyl)-benzo[1,3,2]dioxaborole

Guidance literature:: bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; In benzene-d6; (N2), HBcat in C6D6 reacted with phenyl vinyl sulfide at room temp. catalyzed by (Cp*IrCl2)2 (5 mol%); not isolated, detected by NMR, chromy.;
DOI:10.1016/j.molcata.2007.05.026