1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene

Base Information

• Chemical Name: 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene
• CAS No.: 35502-50-2
• Molecular Formula: C₆₈H₄₆
• Molecular Weight: 863.113
• Mol file: 35502-50-2.mol

Synonyms:

Chemical Property of 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene

There total 2 articles about 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

5,6,9,10-tetrahydrobenzocyclooctene (58150-58-6) + 2,3,4,5-tetraphenylcyclopenta-2,4-dienone (479-33-4) → 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene (35502-50-2)

Guidance literature:

In diethyl ether; for 4h; Heating;

DOI:10.1016/S0040-4020(01)88542-2

Reference yield:

5,10-dibromobenzocyclooctene (17557-54-9) + 2,3,4,5-tetraphenylcyclopenta-2,4-dienone (479-33-4) → 1,2,3,4,9,10,11,12-octaphenyltribenzocyclooctene (35502-50-2)

Guidance literature:

With potassium tert-butylate; In diethyl ether; Heating;

DOI:10.1039/P19720000717

upstream raw materials:

5,6,9,10-tetrahydrobenzocyclooctene

2,3,4,5-tetraphenylcyclopenta-2,4-dienone

5,10-dibromobenzocyclooctene