Technology Process of C45H53NO10
There total 4 articles about C45H53NO10 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at -20 - 20 ℃;
optical yield given as %de;
Molecular sieve;
Inert atmosphere;
DOI:10.1021/jo1016579
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / methanol / 2 h / 70 °C
2: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 - 20 °C / Molecular sieve; Inert atmosphere
With
N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; potassium carbonate;
In
methanol; dichloromethane;
DOI:10.1021/jo1016579
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 20 °C
2: Jones reagent; mercury(II) diacetate / water; acetone / 6 h / 0 °C
3: potassium carbonate / methanol / 2 h / 70 °C
4: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 - 20 °C / Molecular sieve; Inert atmosphere
With
pyridine; N-iodo-succinimide; Jones reagent; trimethylsilyl trifluoromethanesulfonate; mercury(II) diacetate; potassium carbonate;
In
methanol; dichloromethane; water; acetone;
DOI:10.1021/jo1016579
