(-)-(1S,2R,4S)-neodihydrocarvylamine

Base Information

Chemical Name:(-)-(1S,2R,4S)-neodihydrocarvylamine
CAS No.:67690-41-9
Molecular Formula:C₁₀H₁₉N
Molecular Weight:153.268
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(1S,2R,4S)-neodihydrocarvylamine

Chemical Property:

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Technology Process of (-)-(1S,2R,4S)-neodihydrocarvylamine

There total 6 articles about (-)-(1S,2R,4S)-neodihydrocarvylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 89951-92-8
(-)-(1S,2R,4S)-2-azido-trans-p-menth-8⁽¹⁰⁾-en-9-ol

: 67690-41-9
(-)-(1S,2R,4S)-neodihydrocarvylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 3.8 g / LiAlH₄ / diethyl ether / 3 h / Heating

2: 0.25 g / H₂ / Ni-Raney / ethanol / 5 h / 100 °C / 53200 Torr

3: 80 mg / POCl₃, pyridine / 6 h / 45 °C

With pyridine; lithium aluminium tetrahydride; hydrogen; trichlorophosphate; Ni-Raney; In diethyl ether; ethanol;

Reference yield:

: (-)-(1S,2R,4S)-2-azido-8,9-epoxy-trans-p-menthane

: 67690-41-9
(-)-(1S,2R,4S)-neodihydrocarvylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 5.2 g / 1percent aq. H₂SO₄ / 3 h / 0 - 5 °C

2: 1.2 g / POCl₃, pyridine / Ambient temperature

3: 3.8 g / LiAlH₄ / diethyl ether / 3 h / Heating

4: 0.25 g / H₂ / Ni-Raney / ethanol / 5 h / 100 °C / 53200 Torr

5: 80 mg / POCl₃, pyridine / 6 h / 45 °C

With pyridine; lithium aluminium tetrahydride; sulfuric acid; hydrogen; trichlorophosphate; Ni-Raney; In diethyl ether; ethanol;

Reference yield:

: (-)-(1S,2R,4S)-2-azido-trans-p-mentha-8,9-diol

: 67690-41-9
(-)-(1S,2R,4S)-neodihydrocarvylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1.2 g / POCl₃, pyridine / Ambient temperature

2: 3.8 g / LiAlH₄ / diethyl ether / 3 h / Heating

3: 0.25 g / H₂ / Ni-Raney / ethanol / 5 h / 100 °C / 53200 Torr

4: 80 mg / POCl₃, pyridine / 6 h / 45 °C

With pyridine; lithium aluminium tetrahydride; hydrogen; trichlorophosphate; Ni-Raney; In diethyl ether; ethanol;