C₄₉H₇₆N₄O₈Zn

Base Information

• Chemical Name: C₄₉H₇₆N₄O₈Zn
• CAS No.: 1276654-20-6
• Molecular Formula: C₄₉H₇₆N₄O₈Zn
• Molecular Weight: 914.554
• Mol file: 1276654-20-6.mol

Synonyms:

Chemical Property of C₄₉H₇₆N₄O₈Zn

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₉H₇₆N₄O₈Zn

There total 5 articles about C₄₉H₇₆N₄O₈Zn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.1%

C47H74N4O6 (1018968-39-2) + zinc(II) acetate dihydrate (5970-45-6) → C49H76N4O8Zn (1276654-20-6,1016229-16-5)

Guidance literature:

C₄₇H₇₄N₄O₆; In methanol; at 20 ℃;

zinc(II) acetate dihydrate; In methanol; at 20 ℃; for 5h;

Reference yield:

2,6-di-tert-butyl-4-methylcyclohexanol (163119-16-2) → C49H76N4O8Zn (1276654-20-6,1016229-16-5)

Guidance literature:

Multi-step reaction with 5 steps

1.1: pyridine / acetic anhydride; toluene / 4 h / 20 - 30 °C

2.1: sodium methylate / ethanol; water; methanol / 5 - 20 °C / Reflux

3.1: acetic acid / 12 h / 20 °C

4.1: dmap / 1-methyl-pyrrolidin-2-one; acetonitrile / Reflux

4.2: 6 h / Reflux

5.1: methanol / 20 °C

5.2: 5 h / 20 °C

With pyridine; sodium methylate; dmap; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; water; acetic anhydride; acetic acid; toluene; acetonitrile;

Reference yield:

cyanoacetic acid 2,6-di-t-butyl-4-methylcyclohexyl ester (217956-11-1) → C49H76N4O8Zn (1276654-20-6,1016229-16-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: sodium methylate / ethanol; water; methanol / 5 - 20 °C / Reflux

2.1: acetic acid / 12 h / 20 °C

3.1: dmap / 1-methyl-pyrrolidin-2-one; acetonitrile / Reflux

3.2: 6 h / Reflux

4.1: methanol / 20 °C

4.2: 5 h / 20 °C

With sodium methylate; dmap; In 1-methyl-pyrrolidin-2-one; methanol; ethanol; water; acetic acid; acetonitrile;

upstream raw materials:

2,6-di-tert-butyl-4-methylcyclohexanol

C₄₇H₇₄N₄O₆

zinc(II) acetate dihydrate

cyanoacetic acid 2,6-di-t-butyl-4-methylcyclohexyl ester