9-cis-7,8-Didehydroisorenieraten

Base Information

Chemical Name:9-cis-7,8-Didehydroisorenieraten
CAS No.:43161-29-1
Molecular Formula:C₄₀H₄₆
Molecular Weight:526.805
Hs Code.:

Synonyms:

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Chemical Property of 9-cis-7,8-Didehydroisorenieraten

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Technology Process of 9-cis-7,8-Didehydroisorenieraten

There total 11 articles about 9-cis-7,8-Didehydroisorenieraten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2529-36-4
2,3,6-trimethylbenzoic acid

: 43161-29-1,54323-41-0
9-cis-7,8-Didehydroisorenieraten

Guidance literature:: Multi-step reaction with 8 steps

1: SOCl₂

3: collidine, PCl₅

4: NaNH₂ / 160 - 180 °C

5: (i) iPrMgBr, CuCl, (ii) /BRN= 506021/

7: (i) PhLi, (ii) /BRN= 1722399/

8: CH₂Cl₂ / Heating

With 2,3,5-trimethyl-pyridine; thionyl chloride; phosphorus pentachloride; sodium amide; In dichloromethane;
DOI:10.1246/bcsj.47.350

Reference yield:

: 54200-87-2
2,3,6-trimethyl-benzoyl chloride

: 43161-29-1,54323-41-0
9-cis-7,8-Didehydroisorenieraten

Guidance literature:: Multi-step reaction with 7 steps

2: collidine, PCl₅

3: NaNH₂ / 160 - 180 °C

4: (i) iPrMgBr, CuCl, (ii) /BRN= 506021/

6: (i) PhLi, (ii) /BRN= 1722399/

7: CH₂Cl₂ / Heating

With 2,3,5-trimethyl-pyridine; phosphorus pentachloride; sodium amide; In dichloromethane;
DOI:10.1246/bcsj.47.350

Reference yield:

: 54200-88-3
Methyl-3-methyl-5-(2,3,4-trimethylphenyl)-2-trans-4-pentadienoat

: 43161-29-1,54323-41-0
9-cis-7,8-Didehydroisorenieraten

Guidance literature:: Multi-step reaction with 3 steps

1: AlH₃

3: CH₂Cl₂ / Heating

With aluminium hydride; In dichloromethane;
DOI:10.1246/bcsj.47.350