C₃₁H₅₈O₅Si₂

Base Information

Chemical Name:C₃₁H₅₈O₅Si₂
CAS No.:1402820-27-2
Molecular Formula:C₃₁H₅₈O₅Si₂
Molecular Weight:566.97
Hs Code.:

C<sub>31</sub>H<sub>58</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₅₈O₅Si₂

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Technology Process of C₃₁H₅₈O₅Si₂

There total 17 articles about C₃₁H₅₈O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1402820-49-8
C₃₁H₅₆O₅Si₂

: 1402820-27-2
C₃₁H₅₈O₅Si₂

: 1402820-26-1
C₃₁H₅₈O₅Si₂

Guidance literature:: With L-Selectride; In tetrahydrofuran; at -30 ℃; for 6h; optical yield given as %de;
DOI:10.1002/anie.201203935

Reference yield:

: 1402820-25-0
C₂₀H₄₂O₄Si₂

: 90344-49-3
(2R)-3-iodo-2-methylpropyl benzyl ether

: 1402820-27-2
C₃₁H₅₈O₅Si₂

: 1402820-26-1
C₃₁H₅₈O₅Si₂

Guidance literature:: (2R)-3-iodo-2-methylpropyl benzyl ether; With tert.-butyl lithium; In diethyl ether; pentane; at -78 - 20 ℃; for 0.583333h;

C₂₀H₄₂O₄Si₂; In diethyl ether; pentane; at -78 ℃; for 0.5h; optical yield given as %de; diastereoselective reaction;
DOI:10.1002/anie.201203935

Reference yield:

: C₂₅H₅₂O₆Si₂

: 1402820-27-2
C₃₁H₅₈O₅Si₂

: 1402820-26-1
C₃₁H₅₈O₅Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: toluene / 20 h / 100 °C

2.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2.25 h / 95 °C

3.1: lithium aluminium tetrahydride / diethyl ether / 0.5 h / 0 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.2: 0.17 h

5.1: tert.-butyl lithium / diethyl ether; pentane / 0.58 h / -78 - 20 °C

5.2: 0.5 h / -78 °C

With lithium aluminium tetrahydride; oxalyl dichloride; 2,2'-azobis(isobutyronitrile); tert.-butyl lithium; tri-n-butyl-tin hydride; dimethyl sulfoxide; In diethyl ether; dichloromethane; toluene; pentane;
DOI:10.1002/anie.201203935