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Technology Process of (P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O

(P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O

Base Information
  • Chemical Name:(P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O
  • CAS No.:463967-27-3
  • Molecular Formula:C59H50OP2Ru
  • Molecular Weight:938.063
  • Hs Code.:
(P(C<sub>6</sub>H<sub>5</sub>)3)2Ru(C<sub>9</sub>H<sub>7</sub>)CCC(C<sub>6</sub>H<sub>5</sub>)(H)C<sub>5</sub>H<sub>7</sub>O

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Chemical Property of (P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O
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Technology Process of (P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O

There total 1 articles about (P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

[Ru(η(5)-indenyl)(=C=C=C(H)Ph)(triphenylphosphine)2](hexafluorophosphate)

[Ru(η(5)-indenyl)(=C=C=C(H)Ph)(triphenylphosphine)2](hexafluorophosphate)

lithium cyclopent-1-enolate
37160-52-4

lithium cyclopent-1-enolate

(P(C<sub>6</sub>H<sub>5</sub>)3)2Ru(C<sub>9</sub>H<sub>7</sub>)CCC(C<sub>6</sub>H<sub>5</sub>)(H)C<sub>5</sub>H<sub>7</sub>O
463967-27-3,463966-85-0

(P(C6H5)3)2Ru(C9H7)CCC(C6H5)(H)C5H7O

Guidance literature:
In tetrahydrofuran; addn. of THF soln. contg. lithium enolate to THF soln. of Ru complex at -20°C, warming to room temp.; removing solvent in vac., dissolution in dichloromethane, chromy. on silica gel, elution with hexane/diethyl ether mixt. (2:1); elem. anal.;
DOI:10.1021/om0202928
upstream raw materials:

lithium cyclopent-1-enolate

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