3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide

Base Information

Chemical Name:3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide
CAS No.:201216-88-8
Molecular Formula:C₁₉H₁₂ClNO₅W
Molecular Weight:553.611
Hs Code.:

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Chemical Property of 3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide

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Technology Process of 3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide

There total 1 articles about 3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16114-24-2
1-benzyl-3,4-dichloro-pyrrole-2,5-dione

: bis(tricarbonyl(η-cyclopentadienyl)tungsten)

: 201216-88-8
3-chloro-2-(cyclopentadienyltricarbonyltungsta)-N-benzylmaleinimide

Guidance literature:: With Na/Hg; In tetrahydrofuran; N2-atmosphere; addn. of 1% Na-amalgam to W-complex at 0°C, warming to room temp. (after 30 min), stirring for 2 h, cooling to -40°C, dropwise addn. to equimolar amt. of ligand at -78°C, stirring for 12 h, warming to -40°C; solvent removal (vac.), addn. of ether, filtration, evapn., washing (hexane), drying (vac.); elem. anal.;
DOI:10.1016/S0022-328X(96)06647-8