2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

Base Information

Chemical Name:2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene
CAS No.:139097-88-4
Molecular Formula:C₂₅H₁₉BrO₂
Molecular Weight:431.329
Hs Code.:

2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobuta<l>phenanthrene

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Chemical Property of 2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

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Technology Process of 2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

There total 4 articles about 2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 139097-87-3
cis-1-Acetyl-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

: 139097-88-4
2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

Guidance literature:: With N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; for 4h; Heating;

Reference yield:

: 3462-97-3
(4-methoxybenzyl)triphenylphosphonium bromide

: 139097-88-4
2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / 0.4 M aq. LiOH / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 55 percent / CH₂Cl₂ / 576 h / Heating

3: 53 percent / NBS, benzoyl peroxide / CCl₄ / 4 h / Heating

With lithium hydroxide; N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; dichloromethane;

Reference yield:

: 84-11-7
9,10-phenanthrenequinone

: 139097-88-4
2-Acetyl-1-bromo-2-(4-methoxyphenyl)-1,2-dihydrocyclobutaphenanthrene

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / 0.4 M aq. LiOH / CH₂Cl₂ / 0.25 h / Ambient temperature

2: 55 percent / CH₂Cl₂ / 576 h / Heating

3: 53 percent / NBS, benzoyl peroxide / CCl₄ / 4 h / Heating

With lithium hydroxide; N-Bromosuccinimide; Perbenzoic acid; In tetrachloromethane; dichloromethane;