C₂₅H₄₀N₂O₅Si

Base Information

• Chemical Name: C₂₅H₄₀N₂O₅Si
• CAS No.: 1392005-79-6
• Molecular Formula: C₂₅H₄₀N₂O₅Si
• Molecular Weight: 476.688
• Mol file: 1392005-79-6.mol

Synonyms:

Chemical Property of C₂₅H₄₀N₂O₅Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₄₀N₂O₅Si

There total 4 articles about C₂₅H₄₀N₂O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,3-dimethylbutyrylaldehyde (2987-16-8) + C19H30N2O5Si (1392005-77-4) → C25H40N2O5Si (1392005-79-6)

Guidance literature:

With magnesium sulfate; In dichloromethane; at 20 ℃; for 2.5h; Inert atmosphere;

DOI:10.1021/om300442e

Reference yield:

C9H19N3O2Si → C25H40N2O5Si (1392005-79-6)

Guidance literature:

Multi-step reaction with 7 steps

1.1: acetone / 16 h / Inert atmosphere; Reflux

2.1: hydrogenchloride / water / 6 h / Reflux

3.1: sodium hydroxide / water; methanol / 168 h / 20 °C / Inert atmosphere

4.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

5.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

6.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

6.2: Inert atmosphere

7.1: magnesium sulfate / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; chloro-trimethyl-silane; thionyl chloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); magnesium sulfate; sodium hydroxide; phenol; In methanol; dichloromethane; water; acetone;

DOI:10.1021/om300442e

Reference yield:

C9H21NO2Si (1392043-65-0) → C25H40N2O5Si (1392005-79-6)

Guidance literature:

Multi-step reaction with 6 steps

1.1: hydrogenchloride / water / 6 h / Reflux

2.1: sodium hydroxide / water; methanol / 168 h / 20 °C / Inert atmosphere

3.1: thionyl chloride / -20 °C / Inert atmosphere; Reflux

4.1: 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); 4-methyl-morpholine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

5.1: chloro-trimethyl-silane; phenol / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.2: Inert atmosphere

6.1: magnesium sulfate / dichloromethane / 2.5 h / 20 °C / Inert atmosphere

With 4-methyl-morpholine; hydrogenchloride; chloro-trimethyl-silane; thionyl chloride; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); magnesium sulfate; sodium hydroxide; phenol; In methanol; dichloromethane; water;

DOI:10.1021/om300442e

upstream raw materials:

diethyl methyl[(trimethylsilyl)methyl]malonate

C₉H₂₁NO₂Si

3,3-dimethylbutyrylaldehyde

C₁₉H₃₀N₂O₅Si