1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene

Base Information

Chemical Name:1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene
CAS No.:1245505-08-1
Molecular Formula:C₃₂H₄₄N₂PSb
Molecular Weight:609.439
Hs Code.:

Synonyms:

Suppliers and Price of 1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene

There total 1 articles about 1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 312920-30-2
1-chloro-2,3,4,5-tetraethylphosphole

: 811470-79-8
C₂N₂H₂(mesityl)2SbCl

: 1245505-08-1
1,3-di-mesityl-2-(2',3',4',5'-tetraethylphospholyl)-1,3,2-diazastibolene

Guidance literature:: With Li; In tetrahydrofuran; Li reacted with phosphole deriv. in THF; soln. added dropwise to cooled (-78°C) soln. of Sb compd. in THF; mixt. allowed to warm to room temp., stirred for 1 h; solvent removed under reduced pressure, dissolved in hexane; ppt. removed by filtration, vol. reduced to 20 mL, stored at -20°C for crystn.; ppt. collected by filtration, dried in vacuo; elem. anal.;
DOI:10.1002/zaac.200900564