{4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid

Base Information

• Chemical Name: {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid
• CAS No.: 186707-01-7
• Molecular Formula: C₃₈H₄₇IO₁₃P₄
• Molecular Weight: 962.583

Synonyms:

Chemical Property of {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid

There total 3 articles about {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

{4-tert-Butyl-2-[12-tert-butyl-1,6-bis-(diethoxy-phosphorylmethoxy)-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ5-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-7-yl]-6-methyl-benzyl}-phosphonic acid dimethyl ester (186706-99-0) → {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ5-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid (186707-01-7)

Guidance literature:

With trimethylsilyl iodide; In chloroform; for 25h;

DOI:10.1039/P19960002889

Reference yield:

[4-tert-Butyl-2-(12-tert-butyl-1,6-dihydroxy-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ5-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-7-yl)-6-methyl-benzyl]-phosphonic acid dimethyl ester (186706-97-8) → {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ5-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid (186707-01-7)

Guidance literature:

Multi-step reaction with 2 steps

1: NaH, HMPA / benzene / 18 h / 44 °C

2: iodotrimethylsilane / CHCl₃ / 25 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; trimethylsilyl iodide; sodium hydride; In chloroform; benzene;

DOI:10.1039/P19960002889

Reference yield:

Acetic acid 1-acetoxy-12-tert-butyl-7-[5-tert-butyl-2-(dimethoxy-phosphorylmethyl)-3-methyl-phenyl]-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ5-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-6-yl ester (186706-95-6) → {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ5-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid (186707-01-7)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH / methanol / 0.02 h

2: NaH, HMPA / benzene / 18 h / 44 °C

3: iodotrimethylsilane / CHCl₃ / 25 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; trimethylsilyl iodide; sodium hydride; In methanol; chloroform; benzene;

DOI:10.1039/P19960002889

upstream raw materials:

{4-tert-Butyl-2-[12-tert-butyl-1,6-bis-(diethoxy-phosphorylmethoxy)-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ⁵-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-7-yl]-6-methyl-benzyl}-phosphonic acid dimethyl ester

[4-tert-Butyl-2-(12-tert-butyl-1,6-dihydroxy-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ⁵-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-7-yl)-6-methyl-benzyl]-phosphonic acid dimethyl ester

Acetic acid 1-acetoxy-12-tert-butyl-7-[5-tert-butyl-2-(dimethoxy-phosphorylmethyl)-3-methyl-phenyl]-10-methyl-7b-oxo-7bH,9H-8-oxa-7bλ⁵-phospha-benzo[6,7]cyclohepta[1,2,3-jk]fluoren-6-yl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 186707-01-7 {4-tert-Butyl-2-[6-(5-tert-butyl-2-iodomethyl-3-methyl-phenyl)-5-hydroxy-5-oxo-3,7-bis-phosphonomethoxy-5H-5λ⁵-dibenzophosphol-4-yl]-6-methyl-benzyl}-phosphonic acid

Send

Send

Metric Ton KG G Pound L ML

Send

Send