C₁₆H₂₂O₅

Base Information

Chemical Name:C₁₆H₂₂O₅
CAS No.:1360873-03-5
Molecular Formula:C₁₆H₂₂O₅
Molecular Weight:294.348
Hs Code.:

C<sub>16</sub>H<sub>22</sub>O<sub>5</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₂₂O₅

Chemical Property:

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Technology Process of C₁₆H₂₂O₅

There total 1 articles about C₁₆H₂₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₀O₅

: 1360873-03-5
C₁₆H₂₂O₅

Guidance literature:: With platinum(IV) oxide; hydrogen; In ethyl acetate; at 20 ℃; for 1.33333h;
DOI:10.1002/chem.201101437

Reference yield:

: 1360873-03-5
C₁₆H₂₂O₅

: 1206828-93-4
C₁₄H₂₀O₄

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1002/chem.201101437

Reference yield:

: 1360873-03-5
C₁₆H₂₂O₅

: 1028432-85-0
C₅₂H₆₆O₇Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Reflux

3.1: 20% palladium hydroxide on charcoal; hydrogen / ethyl acetate / 10 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.58 h / 0 - 20 °C

4.2: 14.08 h / 0 - 20 °C

5.1: hydrogenchloride / methanol; water / 29 h / 20 °C

6.1: 2,2,6,6-tetramethyl-piperidine-N-oxyl; [bis(acetoxy)iodo]benzene / dichloromethane / 45 h / 20 °C

7.1: N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane / tetrahydrofuran; toluene / 2.33 h / -78 °C

8.1: tert.-butyl lithium; 9-methoxy-9-BBN / tetrahydrofuran; diethyl ether; hexane; pentane / 1.17 h / -78 - 20 °C

8.2: 50 °C

9.1: 2,3-Dimethyl-2-butene; dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

9.2: 0 - 20 °C

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; 2,2,6,6-tetramethyl-piperidine-N-oxyl; lithium aluminium tetrahydride; 2,3-Dimethyl-2-butene; [bis(acetoxy)iodo]benzene; dimethylsulfide borane complex; 20% palladium hydroxide on charcoal; hydrogen; tert.-butyl lithium; potassium hexamethylsilazane; sodium hydride; N-ethyl-N,N-diisopropylamine; 9-methoxy-9-BBN; In tetrahydrofuran; methanol; diethyl ether; hexane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene; mineral oil; pentane; 8.2: Suzuki-Miyaura coupling;
DOI:10.1002/chem.201101437