(C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl

Base Information

Chemical Name:(C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl
CAS No.:179676-06-3
Molecular Formula:C₁₃H₁₇ClHgN₂O
Molecular Weight:453.334
Hs Code.:

(C<sub>6</sub>H<sub>3</sub>(C<sub>3</sub>H<sub>2</sub>NO(CH<sub>3</sub>)2)(N(CH<sub>3</sub>)2))HgCl

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Chemical Property of (C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl

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Technology Process of (C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl

There total 1 articles about (C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 176324-83-7
4-(4,4-dimethyl-2-oxazolin-2-yl)-N,N-dimethylaniline

: mercury dichloride

: 179676-06-3
(C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl

Guidance literature:: With n-butyllithium; In not given; N2-atmosphere; addn. of BuLi (in hexane) to ligand precursor (in Et2O orTHF, not specified) at 0°C, stirring at 0°C for 4 h, drop wise addn. of stoich. amt. HgCl2 at -78°C, stirring at room temp.for 5 h; filtration, evapn., recrystn. (Et2O or Et2O/CH2Cl2=2:1, not specified); elem. anal.;
DOI:10.1016/0022-328X(95)06081-7

Reference yield:

: 179676-06-3
(C₆H₃(C₃H₂NO(CH₃)2)(N(CH₃)2))HgCl

: 181886-23-7
C₆H₃(N(CH₃)2)(C₅H₈NO)AuCl(P(C₆H₅)3)⁽¹⁺⁾*Cl^(1-) = [C₆H₃(N(CH₃)2)(C₅H₈NO)AuCl(P(C₆H₅)3)]Cl

Guidance literature:: Multi-step reaction with 2 steps

1: tetramethylammonium chloride / acetonitrile

2: dichloromethane

With tetramethylammonium chloride; In dichloromethane; acetonitrile;
DOI:10.1039/dt9960003185