Ge(((CH₃)2CH)2C₆H₃NCHNC₆H₃(CH(CH₃)2)2)2

Base Information

• Chemical Name: Ge(((CH₃)2CH)2C₆H₃NCHNC₆H₃(CH(CH₃)2)2)2
• CAS No.: 1037079-26-7
• Molecular Formula: C₅₀H₇₀GeN₄
• Molecular Weight: 799.723
• Mol file: 1037079-26-7.mol

Synonyms:

Chemical Property of Ge(((CH₃)2CH)2C₆H₃NCHNC₆H₃(CH(CH₃)2)2)2

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of Ge(((CH₃)2CH)2C₆H₃NCHNC₆H₃(CH(CH₃)2)2)2

There total 1 articles about Ge(((CH₃)2CH)2C₆H₃NCHNC₆H₃(CH(CH₃)2)2)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

germanium(II) chloride dioxane + N,N'-di(2,6-diisopropylphenyl)formamidine (1176938-29-6,581776-24-1) → Ge(((CH3)2CH)2C6H3NCHNC6H3(CH(CH3)2)2)2 (1037079-26-7)

Guidance literature:

With n-BuLi; In diethyl ether; hexane; byproducts: LiCl; under Ar or N2; soln. of n-BuLi in hexanes added to soln. of ligand in Et2O at 20°C; stirred overnight; added at -80°C to slurry of GeCl2*(dioxane) in Et2O over 5 min; warmed to room temp. over 4 h; volatiles removed in vac.; extd. into toluene; crystd. at 4°C;

DOI:10.1039/b801168k

upstream raw materials:

N,N'-di(2,6-diisopropylphenyl)formamidine