1,2-Cyclobutanedimethanol, dimethanesulfonate, trans-

Base Information

Chemical Name:1,2-Cyclobutanedimethanol, dimethanesulfonate, trans-
CAS No.:139506-15-3
Molecular Formula:C8H16O6S2
Molecular Weight:272.343
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Cyclobutanedimethanol, dimethanesulfonate, trans-

Chemical Property:

Purity/Quality:

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Technology Process of 1,2-Cyclobutanedimethanol, dimethanesulfonate, trans-

There total 1 articles about 1,2-Cyclobutanedimethanol, dimethanesulfonate, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4462-96-8
cis-1,2-cyclobutane dicarboxylic anhydride

: 139506-15-3
cis-1,2-bis(hydroxymethyl)cyclobutane dimesylate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1.25 h / 0 °C / Inert atmosphere

2: triethylamine / dichloromethane / -15 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jacs.6b10706

Reference yield:

: 139506-15-3
cis-1,2-bis(hydroxymethyl)cyclobutane dimesylate

: 2235-12-3
1,3,5-hexatriene

: 1165952-91-9
cyclohexa-1,3-diene

Guidance literature:: Multi-step reaction with 5 steps

1: sodiumsulfide nonahydrate / ethanol; water / 12 h / Inert atmosphere; Reflux

2: sulfuric acid; dihydrogen peroxide / isopropyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3: pyridine; sulfuryl dichloride / dichloromethane / 1 h / -40 °C / Inert atmosphere

4: potassium tert-butylate / dimethyl sulfoxide / 15 h / 0 - 20 °C / Inert atmosphere

5: copper(I) trifluoromethanesulfonate benzene / diethyl ether / 27 °C / Inert atmosphere; UV-irradiation

With pyridine; sulfuryl dichloride; copper(I) trifluoromethanesulfonate benzene; sodiumsulfide nonahydrate; sulfuric acid; potassium tert-butylate; dihydrogen peroxide; In diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; 4: |Ramberg-Baecklund-Paquette Olefin Synthesis;
DOI:10.1021/jacs.6b10706

Reference yield:

: 139506-15-3
cis-1,2-bis(hydroxymethyl)cyclobutane dimesylate

: [5]-ladderane

: 1165952-91-9
cyclohexa-1,3-diene

Guidance literature:: Multi-step reaction with 5 steps

1: sodiumsulfide nonahydrate / ethanol; water / 12 h / Inert atmosphere; Reflux

2: sulfuric acid; dihydrogen peroxide / isopropyl alcohol / 16 h / 0 - 20 °C / Inert atmosphere

3: pyridine; sulfuryl dichloride / dichloromethane / 1 h / -40 °C / Inert atmosphere

4: potassium tert-butylate / dimethyl sulfoxide / 15 h / 0 - 20 °C / Inert atmosphere

5: copper(I) trifluoromethanesulfonate benzene / benzene / 60 h / -4 °C / Inert atmosphere; UV-irradiation

With pyridine; sulfuryl dichloride; copper(I) trifluoromethanesulfonate benzene; sodiumsulfide nonahydrate; sulfuric acid; potassium tert-butylate; dihydrogen peroxide; In ethanol; dichloromethane; water; dimethyl sulfoxide; isopropyl alcohol; benzene; 4: |Ramberg-Baecklund-Paquette Olefin Synthesis;
DOI:10.1021/jacs.6b10706