C₇H₁₀N₂*C₂₂H₂₁BrO₄

Base Information

Chemical Name:C₇H₁₀N₂*C₂₂H₂₁BrO₄
CAS No.:1314608-64-4
Molecular Formula:C₇H₁₀N₂*C₂₂H₂₁BrO₄
Molecular Weight:551.48
Hs Code.:

C<sub>7</sub>H<sub>10</sub>N<sub>2</sub>*C<sub>22</sub>H<sub>21</sub>BrO<sub>4</sub>

Synonyms:

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Chemical Property of C₇H₁₀N₂*C₂₂H₂₁BrO₄

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Technology Process of C₇H₁₀N₂*C₂₂H₂₁BrO₄

There total 6 articles about C₇H₁₀N₂*C₂₂H₂₁BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1001019-63-1
(5R,6S,E)-methyl 6-(2-bromophenyl)-6-methoxy-5-methylhex-3-enoate

: 1314608-64-4
C₇H₁₀N₂*C₂₂H₂₁BrO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 8 h / 0 - 20 °C

2.1: Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4 / toluene / 24 h / -50 - -40 °C / Inert atmosphere

3.1: lithium hydroxide / tetrahydrofuran; methanol; water / 48 h / 20 °C / Inert atmosphere

3.2: Inert atmosphere

4.1: diethyl ether / 12 h / 20 °C / Inert atmosphere

With Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; water; toluene; acetonitrile;
DOI:10.1002/anie.201101366

Reference yield:

: C₁₅H₂₂O₂Si

: 1314608-64-4
C₇H₁₀N₂*C₂₂H₂₁BrO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 16 h / -78 °C / Inert atmosphere

2.1: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 8 h / 0 - 20 °C

3.1: Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4 / toluene / 24 h / -50 - -40 °C / Inert atmosphere

4.1: lithium hydroxide / tetrahydrofuran; methanol; water / 48 h / 20 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: diethyl ether / 12 h / 20 °C / Inert atmosphere

With Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4; trimethylsilyl trifluoromethanesulfonate; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/anie.201101366

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 1314608-64-4
C₇H₁₀N₂*C₂₂H₂₁BrO₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 16 h / -78 °C / Inert atmosphere

2.1: 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 8 h / 0 - 20 °C

3.1: Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4 / toluene / 24 h / -50 - -40 °C / Inert atmosphere

4.1: lithium hydroxide / tetrahydrofuran; methanol; water / 48 h / 20 °C / Inert atmosphere

4.2: Inert atmosphere

5.1: diethyl ether / 12 h / 20 °C / Inert atmosphere

With Rh₂[(N-(4-dodecylphenyl)sulfonyl)-(S)-prolinate]4; trimethylsilyl trifluoromethanesulfonate; 4-acetamidobenzenesulfonyl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/anie.201101366