[((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

Base Information

Chemical Name:[((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]
CAS No.:831193-25-0
Molecular Formula:C₂₁H₂₉ClN₂Si₂Sn
Molecular Weight:519.809
Hs Code.:

[((CH<sub>3</sub>)3SiNC(C<sub>6</sub>H<sub>5</sub>)CHC(C<sub>6</sub>H<sub>5</sub>)NSi(CH<sub>3</sub>)3)SnCl]

Synonyms:

Suppliers and Price of [((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

There total 1 articles about [((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2Li⁽¹⁺⁾*2(N(Si(CH₃)3)C(C₆H₅))2CH^(1-)=(Li((N(Si(CH₃)3)C(C₆H₅))2CH))2

: tin(ll) chloride

: 831193-25-0
[((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

Guidance literature:: In diethyl ether; (Ar); Schlenk technique; soln. of Li compd. in Et2O was slowly added to stirred suspn. of SnCl2 in Et2O at room temp.; suspn. was stirred for 13h; filtered; solvent from filtrate removed (vac.); residue washed (light petroleum ether); elem. anal.;
DOI:10.1039/b412765j

Reference yield: 87.0%

: 831193-25-0
[((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnCl]

: 1070-89-9
sodium hexamethyldisilazane

: 831193-40-9
[((CH₃)3SiNC(C₆H₅)CHC(C₆H₅)NSi(CH₃)3)SnN(Si(CH₃)3)2]

Guidance literature:: In diethyl ether; (Ar); Schlenk technique; amide was added to stirred soln. of Sn compd. in Et2O at -30°C; mixt. was stirred for 3 h; filtered; solvent removed (vac.); stripped with light petroleum; dissolved in hot C6H6, placed in Dewar vessel filled with hot H2O; slowly cooled for 3 d; elem. anal.;
DOI:10.1039/b412765j