Technology Process of C38H36INO6S
There total 2 articles about C38H36INO6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Iodine monochloride;
In
dichloromethane; acetonitrile;
at 25 ℃;
DOI:10.1021/ic201446x
- Guidance literature:
-
Multi-step reaction with 6 steps
1: tri-tert-butyl phosphine; potassium tert-butylate; bis(dibenzylideneacetone)-palladium(0) / toluene / 80 °C
2: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / Reflux
4: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene / Reflux
6: Iodine monochloride / dichloromethane; acetonitrile / 25 °C
With
tetrakis(triphenylphosphine) palladium(0); tri-tert-butyl phosphine; potassium tert-butylate; Iodine monochloride; sodium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
dichloromethane; water; toluene; acetonitrile;
3: Suzuki coupling / 5: Suzuki coupling;
DOI:10.1021/ic201446x
- Guidance literature:
-
With
tri-tert-butyl phosphine; caesium carbonate; bis(dibenzylideneacetone)-palladium(0);
In
1,4-dioxane;
at 60 ℃;
DOI:10.1021/ic201446x