2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

Base Information

Chemical Name:2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole
CAS No.:79994-76-6
Molecular Formula:C₁₂H₁₁N₃O
Molecular Weight:213.239
Hs Code.:

Synonyms:

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Chemical Property of 2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

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Technology Process of 2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

There total 4 articles about 2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 345228-09-3
2-Amino-1-benzyl-4-methyl-5-phenyl-1,2-dihydro-pyrazol-3-one

: 79994-76-6
2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / acetic acid / 1 h / 100 °C

2: H₂ / Pd/C / acetic acid; ethanol / 760 Torr / Ambient temperature

3: 60 percent / POCl₃, triethylamine / 0.25 h / 100 °C

With hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol; acetic acid;

Reference yield:

: 79994-57-3
1-acetylamino-2-benzyl-4-methyl-3-phenylpyrazolin-5-one

: 79994-76-6
2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd/C / acetic acid; ethanol / 760 Torr / Ambient temperature

2: 60 percent / POCl₃, triethylamine / 0.25 h / 100 °C

With hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In ethanol; acetic acid;

Reference yield:

: 1-benzyl-4-methyl-5-phenylpyrazolin-3-one sodium salt

: 79994-76-6
2,7-dimethyl-6-phenylpyrazolo<3,2-b>-1,3,4-oxadiazole

Guidance literature:: Multi-step reaction with 4 steps

1: 33 percent / chloramine / dimethylformamide; diethyl ether / 12 h / Ambient temperature

2: 45 percent / acetic acid / 1 h / 100 °C

3: H₂ / Pd/C / acetic acid; ethanol / 760 Torr / Ambient temperature

4: 60 percent / POCl₃, triethylamine / 0.25 h / 100 °C

With chloroamine; hydrogen; triethylamine; trichlorophosphate; palladium on activated charcoal; In diethyl ether; ethanol; acetic acid; N,N-dimethyl-formamide;