[Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

Base Information

Chemical Name:[Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]
CAS No.:1357616-35-3
Molecular Formula:C₂₃H₄₇Ir₂O₃P₄*C₃₂H₁₂BF₂₄
Molecular Weight:1743.18
Hs Code.:

Synonyms:

Suppliers and Price of [Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

There total 2 articles about [Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 75-02-5,24981-14-4
1-fluoroethylene

: 1357616-33-1
[Ir2H(CO)2(μ-CO)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

: 1357616-35-3
[Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

: 1357616-37-5
[Ir2(H)2(CO)2(μ-H)(μ-CCHF)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

Guidance literature:: In dichloromethane-d2; (Ar); using Schlenk techniques; charging of NMR tube with (Ir2(CO)3(H)(PEt2CH2PEt2)2)(B((CF3)2C6H3)4), addn. of CD2Cl2, addn. of CFHCH2 via a gastight syringe, vigorous mixing for 30 min; monitoring by NMR, transferring to Schlenk tube, removal of solvent under vac., redissolving in Et2O, addn. of pentane, pptn.; elem. anal.;
DOI:10.1021/om2011968

Reference yield:

: 75-02-5,24981-14-4
1-fluoroethylene

: 1357616-33-1
[Ir2H(CO)2(μ-CO)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

: 1357616-35-3
[Ir2(H)(CO)3(μ-CCH2)(bis(diethylphosphino)methane)2][B(3,5-(CF3)2C6H3)4]

Guidance literature:: With water; In dichloromethane-d2; (Ar); using Schlenk techniques; treatment of (Ir2(CO)3(H)(PEt2CH2PEt2)2)(B((CF3)2C6H3)4) with vinyl fluoride in the presence water (5 equiv.) for 10 min;
DOI:10.1021/om2011968