4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

Base Information

Chemical Name:4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone
CAS No.:1313021-98-5
Molecular Formula:C₁₇H₂₁NO
Molecular Weight:255.36
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

Chemical Property:

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Technology Process of 4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

There total 4 articles about 4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1106767-77-4
4-azido-3,4-dihydro-2H-naphthalen-1-one

: 1313021-98-5
4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

Guidance literature:: Multi-step reaction with 4 steps

1: palladium 10% on activated carbon; hydrogen / ethanol; ethyl acetate / 20 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

3: triethylamine / dichloromethane / 20 °C

4: potassium carbonate / acetone

With palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; In ethanol; dichloromethane; ethyl acetate; acetone;
DOI:10.2174/157340611795564222

Reference yield:

: 1313021-93-0
tert-butyl N-(4-oxo-1,2,3,4-tetrahydro-1-naphthalenyl)carbamate

: 1313021-98-5
4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

Guidance literature:: Multi-step reaction with 3 steps

1: trifluoroacetic acid / dichloromethane / 0 - 20 °C

2: triethylamine / dichloromethane / 20 °C

3: potassium carbonate / acetone

With potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; acetone;
DOI:10.2174/157340611795564222

Reference yield:

: 64833-49-4,61895-10-1
4-amino-3,4-dihydro-2H-naphthalen-1-one

: 1313021-98-5
4-[2-cyclohexenyl(methyl)amino]-1,2,3,4-tetrahydro-1-naphthalenone

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 20 °C

2: potassium carbonate / acetone

With potassium carbonate; triethylamine; In dichloromethane; acetone;
DOI:10.2174/157340611795564222