1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Base Information

Chemical Name:1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene
CAS No.:102393-28-2
Molecular Formula:C₃₄H₄₈N₂O₂
Molecular Weight:516.767
Hs Code.:

Synonyms:

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Chemical Property of 1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Chemical Property:

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Technology Process of 1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

There total 21 articles about 1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102393-16-8
1,4-bis<5-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

: 102393-28-2
1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 98.1 percent / PhCH₂ONa / Heating

2: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

3: dimethylformamide / Heating

4: POCl₃ / CH₂Cl₂ / 0.5 h

5: NaHCO₃ / H₂O / Heating

With hydrogen; sodium hydrogencarbonate; triethylamine; sodium phenyl-methanolate; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 102393-19-1
1,4-bis<5-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

: 102393-28-2
1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 4 steps

1: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

2: dimethylformamide / Heating

3: POCl₃ / CH₂Cl₂ / 0.5 h

4: NaHCO₃ / H₂O / Heating

With hydrogen; sodium hydrogencarbonate; triethylamine; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 3022-16-0
1,4-bis(chloromethyl)-2,3,5,6-tetramethylbenzene

: 102393-28-2
1,4-bis<5-(5-formyl-2,4-dimethylpyrrol-3-yl)pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 17 steps

1: 1.) Na / 1.) ethanol; 2.) ethanol, reflux, 0.5 h

2: H₂O, KOH / Heating

3: 94.7 percent / quinoline / 0.33 h / Heating

4: 89.4 percent / cc. H₂SO₄ / toluene

5: 89.6 percent / B₂H₆ / tetrahydrofuran

6: 91.2 percent / 48 percent HBr / H₂O / 0.5 h / Heating

7: 1.) Na / 1.) ethanol; 2.) ethanol, reflux

8: H₂O, KOH / Heating

9: 94.6 percent / quinoline / 0.33 h / Heating

10: SOCl₂ / Heating

11: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

12: 88.3 percent / B₂H₆ / tetrahydrofuran

13: 98.1 percent / PhCH₂ONa / Heating

14: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

15: dimethylformamide / Heating

16: POCl₃ / CH₂Cl₂ / 0.5 h

17: NaHCO₃ / H₂O / Heating

With quinoline; potassium hydroxide; thionyl chloride; sulfuric acid; water; hydrogen bromide; hydrogen; sodium; sodium hydrogencarbonate; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;