C₃₃H₄₄N₂O₃

Base Information

Chemical Name:C₃₃H₄₄N₂O₃
CAS No.:939442-47-4
Molecular Formula:C₃₃H₄₄N₂O₃
Molecular Weight:516.724
Hs Code.:

C<sub>33</sub>H<sub>44</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₃₃H₄₄N₂O₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₄₄N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₄₄N₂O₃

There total 8 articles about C₃₃H₄₄N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1577-22-6
5-hexenoic acid

: C₂₇H₃₆N₂O₂

: 939442-47-4
C₃₃H₄₄N₂O₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 23 ℃;
DOI:10.1016/j.bmcl.2013.05.028

Reference yield:

: (3-bromobenzyl)magnesium bromide

: 939442-47-4
C₃₃H₄₄N₂O₃

Guidance literature:: Multi-step reaction with 8 steps

1: diethyl ether; dichloromethane / -78 °C

2: tetramethylammonium triacetoxyborohydride / dichloromethane; acetic acid / 23 °C

3: 1,3-dimethylbarbituric acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / dichloromethane / 23 °C

4: dichloromethane / 23 °C

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / Reflux

6: ethanol / 70 °C

7: hydrogenchloride / 1,4-dioxane; dichloromethane / 23 °C

8: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 23 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; potassium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide; 5: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.05.028

Reference yield:

: 1391538-82-1,1217801-96-1
C₁₅H₂₀BrNO₃

: 939442-47-4
C₃₃H₄₄N₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran / Reflux

2: ethanol / 70 °C

3: hydrogenchloride / 1,4-dioxane; dichloromethane / 23 °C

4: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 23 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane; N,N-dimethyl-formamide; 1: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2013.05.028