C₂₃H₂₆O₄

Base Information

Chemical Name:C₂₃H₂₆O₄
CAS No.:1447728-84-8
Molecular Formula:C₂₃H₂₆O₄
Molecular Weight:366.457
Hs Code.:

C<sub>23</sub>H<sub>26</sub>O<sub>4</sub>

Synonyms:

Suppliers and Price of C₂₃H₂₆O₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₆O₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₆O₄

There total 7 articles about C₂₃H₂₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1447728-68-8
C₁₄H₂₀Se

: 1447728-84-8
C₂₃H₂₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

3: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

4: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

5: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 27 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium benzoate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; palladium diacetate; lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 4442-79-9
cyclohexylethan-1-ol

: 1447728-84-8
C₂₃H₂₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1: triethylamine / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

4: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

5: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

6: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

7: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 27 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium benzoate; sodium tetrahydroborate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; palladium diacetate; lithium; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114

Reference yield:

: 75646-21-8
methanesulfonic acid 2-cyclohexyl-ethyl ester

: 1447728-84-8
C₂₃H₂₆O₄

Guidance literature:: Multi-step reaction with 6 steps

1: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

3: sodium benzoate / toluene / 1 h / 100 °C / Inert atmosphere

4: Phenylselenyl bromide / dichloromethane / 5 h / -45 - 0 °C / Inert atmosphere

5: lithium; naphthalene; trimethylsilyl bromide / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere; Sonication

6: palladium diacetate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane / 27 h / 20 °C / Inert atmosphere

With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; sodium benzoate; sodium tetrahydroborate; naphthalene; trimethylsilyl bromide; Phenylselenyl bromide; palladium diacetate; lithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane; toluene;
DOI:10.1016/j.tetlet.2013.05.114