C₂₇H₂₃F₂IN₄O₅

Base Information

Chemical Name:C₂₇H₂₃F₂IN₄O₅
CAS No.:1386374-41-9
Molecular Formula:C₂₇H₂₃F₂IN₄O₅
Molecular Weight:648.405
Hs Code.:

C<sub>27</sub>H<sub>23</sub>F<sub>2</sub>IN<sub>4</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₂₇H₂₃F₂IN₄O₅

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Technology Process of C₂₇H₂₃F₂IN₄O₅

There total 3 articles about C₂₇H₂₃F₂IN₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1620134-10-2
C₂₈H₂₃F₂IN₄O₆

: 1386374-41-9
C₂₇H₂₃F₂IN₄O₅

Guidance literature:: With [bis(acetoxy)iodo]benzene; water; In dichloromethane; ethyl acetate; at 0 ℃; for 2h;
DOI:10.1016/j.bmcl.2014.05.097

Reference yield:

: C₂₂H₁₉FIN₃O₇

: 1386374-41-9
C₂₇H₂₃F₂IN₄O₅

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 2 h / 50 °C

2: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 25 °C

3: [bis(acetoxy)iodo]benzene; water / dichloromethane; ethyl acetate / 2 h / 0 °C

With dmap; [bis(acetoxy)iodo]benzene; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane; water; ethyl acetate; 3: |Hofmann Rearrangement;
DOI:10.1016/j.bmcl.2014.05.097

Reference yield:

: 1620134-05-5
C₂₁H₁₇FIN₃O₇

: 140-75-0
para-fluorobenzylamine

: 1386374-41-9
C₂₇H₂₃F₂IN₄O₅

Guidance literature:: Multi-step reaction with 2 steps

1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 12 h / 25 °C

2: [bis(acetoxy)iodo]benzene; water / dichloromethane; ethyl acetate / 2 h / 0 °C

With dmap; [bis(acetoxy)iodo]benzene; water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; ethyl acetate; 2: |Hofmann Rearrangement;
DOI:10.1016/j.bmcl.2014.05.097