Technology Process of C25H28O3S
There total 14 articles about C25H28O3S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) n-BuLi / 1) THF, hexane, -78 deg C, 1 h
2: 91 percent / Zn(BH4)2 / CH2Cl2; diethyl ether / -78 °C
3: tetrabutylammonium fluoride monohydrate / tetrahydrofuran / Ambient temperature
4: 1) NaH, 2) tetrabutylammonium iodide / 1) THF, 0 deg C, 30 min, 2) reflux, overnight
With
n-butyllithium; zinc(II) tetrahydroborate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)80909-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1) n-BuLi / 1) THF, hexane, -78 deg C, 1 h
2: Zn(BH4)2 / CH2Cl2; diethyl ether / -78 °C
3: tetrabutylammonium fluoride monohydrate / tetrahydrofuran / Ambient temperature
4: 1) NaH, 2) tetrabutylammonium iodide / 1) THF, 0 deg C, 30 min, 2) reflux, overnight
With
n-butyllithium; zinc(II) tetrahydroborate; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(01)80909-1
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1) n-BuLi / 1) THF, hexane, -78 deg C, 1 h
2: DIBAL-H / CH2Cl2; hexane / -78 °C
3: 1) NaH, 2) tetrabutylammonium iodide / 1) THF, 0 deg C, 30 min, 2) reflux, overnight
With
n-butyllithium; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride;
In
hexane; dichloromethane;
DOI:10.1016/S0040-4020(01)80909-1
