Technology Process of C24H20ClN3O6S
There total 6 articles about C24H20ClN3O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methoxybenzene; trifluoroacetic acid;
In
dichloromethane;
at 0 ℃;
for 2h;
DOI:10.1016/j.bmcl.2011.01.132
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C
2: potassium carbonate / N,N-dimethyl-formamide / 70 °C
3: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C
4: pyridine / dichloromethane / 0 - 20 °C
5: methoxybenzene; trifluoroacetic acid / dichloromethane / 2 h / 0 °C
With
pyridine; palladium 10% on activated carbon; tetrabutyl ammonium fluoride; hydrogen; potassium carbonate; methoxybenzene; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.132
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 3 h / 20 °C
2: pyridine / dichloromethane / 0 - 20 °C
3: methoxybenzene; trifluoroacetic acid / dichloromethane / 2 h / 0 °C
With
pyridine; palladium 10% on activated carbon; hydrogen; methoxybenzene; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.01.132
