All-trans-N-retinyliden-n-butylamin

Base Information

• Chemical Name: All-trans-N-retinyliden-n-butylamin
• CAS No.: 66855-42-3
• Molecular Formula: C₂₄H₃₇N
• Molecular Weight: 339.564
• Mol file: 66855-42-3.mol

Synonyms:

Chemical Property of All-trans-N-retinyliden-n-butylamin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of All-trans-N-retinyliden-n-butylamin

There total 3 articles about All-trans-N-retinyliden-n-butylamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-fomyl crotonic acid butyl ester (40212-97-3) → All-trans-N-retinyliden-n-butylamin (66855-42-3)

Guidance literature:

Multi-step reaction with 2 steps

2: B(OnBu)3 / ethyl acetate

With boric acid tributyl ester; In ethyl acetate;

DOI:10.1248/cpb.26.925

Reference yield:

Methyl-β-ionylidenacetat (5300-00-5,7444-27-1,14538-58-0,20110-08-1,22326-58-5,40244-48-2,40244-65-3) → All-trans-N-retinyliden-n-butylamin (66855-42-3)

Guidance literature:

Multi-step reaction with 3 steps

1: ethanol / Irradiation

3: B(OnBu)3 / ethyl acetate

With boric acid tributyl ester; In ethanol; ethyl acetate;

DOI:10.1248/cpb.26.925

Reference yield:

Methyl Retro-γ-ionylideneacetate (66855-39-8) → All-trans-N-retinyliden-n-butylamin (66855-42-3)

Guidance literature:

Multi-step reaction with 2 steps

2: B(OnBu)3 / ethyl acetate

With boric acid tributyl ester; In ethyl acetate;

DOI:10.1248/cpb.26.925

upstream raw materials:

3-fomyl crotonic acid butyl ester

Methyl-β-ionylidenacetat

Methyl Retro-γ-ionylideneacetate