C₁₅H₂₁NO

Base Information

Chemical Name:C₁₅H₂₁NO
CAS No.:1620643-53-9
Molecular Formula:C₁₅H₂₁NO
Molecular Weight:231.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₁NO

Chemical Property:

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Safty Information:

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Technology Process of C₁₅H₂₁NO

There total 2 articles about C₁₅H₂₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 169105-68-4
(2S,4S)-5-benzyloxy-2,4-dimethyl-pentan-1-ol

: 1620643-53-9
C₁₅H₂₁NO

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 13 h / 0 - 20 °C / Inert atmosphere

2: dimethyl sulfoxide / 39 h / 20 °C / Inert atmosphere

With 1H-imidazole; iodine; triphenylphosphine; In diethyl ether; dimethyl sulfoxide; acetonitrile;
DOI:10.1002/anie.201400305

Reference yield:

: 773837-37-9
sodium cyanide

: 1620643-52-8
C₁₄H₂₁IO

: 1620643-53-9
C₁₅H₂₁NO

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 39h; Inert atmosphere;
DOI:10.1002/anie.201400305

Reference yield:

: 1620643-53-9
C₁₅H₂₁NO

: C₄₃H₇₄O₉Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 2 h / 20 °C / Inert atmosphere

2.1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / dichloromethane; hexane / 3 h / -78 °C / Inert atmosphere

4.1: propionic acid; pyrrolidine / water; isopropyl alcohol / 18 h / 55 °C / Inert atmosphere

5.1: cerium(III) chloride heptahydrate / ethanol / 0.5 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 °C / Inert atmosphere

6.1: 1H-imidazole / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere

7.1: tert.-butyl lithium / diethyl ether; pentane / 0.08 h / -78 °C / Inert atmosphere

7.2: 4 h / 20 °C / Inert atmosphere

8.1: Schwartz's reagent / benzene / 24 h / 20 °C / Inert atmosphere

8.2: 1 h

8.3: 20 h / 20 °C / Darkness

9.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere

9.2: 1 h / 20 °C / Inert atmosphere

10.1: pyridinium p-toluenesulfonate / methanol; tetrahydrofuran / 16 h / 20 - 40 °C / Inert atmosphere

11.1: pyridine / 2 h / 0 - 20 °C / Inert atmosphere

With pyrrolidine; pyridine; 1H-imidazole; Schwartz's reagent; chloro-trimethyl-silane; cerium(III) chloride heptahydrate; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; sodium hydride; diisobutylaluminium hydride; propionic acid; triphenylphosphine; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; ethanol; hexane; dichloromethane; water; isopropyl alcohol; acetonitrile; mineral oil; pentane; benzene; 8.3: |Suzuki-Miyaura Coupling;
DOI:10.1002/anie.201400305