Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one

Base Information

Chemical Name:Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one
CAS No.:294174-13-3
Molecular Formula:C₁₈H₉N₃O
Molecular Weight:283.289
Hs Code.:
UNII:Q4EZU6OLN3
Nikkaji Number:J1.639.336C
Wikidata:Q27286992
ChEMBL ID:CHEMBL322742

Synonyms:CRL-8299;UNII-Q4EZU6OLN3;Q4EZU6OLN3;Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one;8H-Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one;294174-13-3;CHEMBL322742;SCHEMBL7186247;ZDXOEMYOODQSEU-UHFFFAOYSA-N;benzo[b]pyrido[4,3,2-de][1,7]phenanthroline-8-one;Q27286992;8H-Benzo[b]pyrido[4,3,2-de][1,7]phenanthroline-8-one

Suppliers and Price of Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:283.074561919
Heavy Atom Count:22
Complexity:467

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C4C(=N2)C5=C(C(=O)C4=NC=C3)N=CC=C5

Technology Process of Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one

There total 5 articles about Benzo(b)pyrido(4,3,2-de)(1,7)phenanthrolin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 294174-02-0
4-(2-trifluoroacetamidophenyl)pyrido[3,2-g]quinoline-5,10-dione

: 294174-13-3
benzo[b]pyrido[4,3,2-de][1,7]phenanthroline-8-one

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 3h; Heating;
DOI:10.1021/jm0108496

Reference yield: 80.0%

: 294174-13-3
benzo[b]pyrido[4,3,2-de][1,7]phenanthroline-8-one

Guidance literature:

Reference yield:

: 10470-83-4
5,8-quinolinedione

: 294174-13-3
benzo[b]pyrido[4,3,2-de][1,7]phenanthroline-8-one

Guidance literature:: Multi-step reaction with 3 steps

1: acetic anhydride / acetonitrile / 24 h / Heating

2: 10percent Pd/C / toluene / 12 h / Heating

3: 80 percent / CF₃COOH / CH₂Cl₂ / 3 h / Heating

With acetic anhydride; trifluoroacetic acid; 10percent Pd/C; In dichloromethane; toluene; acetonitrile; 1: Diels-Alder reaction;
DOI:10.1021/jm0108496