Technology Process of C24H24N2O7
There total 8 articles about C24H24N2O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chloro-trimethyl-silane
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
dmap; chloro-trimethyl-silane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.10.056
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-chloro-succinimide / N,N-dimethyl-formamide / 5 h / 20 °C
2: triethylamine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
dmap; N-chloro-succinimide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.10.056
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydroxylamine hydrochloride; sodium acetate / methanol; water / 12 h / 20 °C
2: N-chloro-succinimide / N,N-dimethyl-formamide / 5 h / 20 °C
3: triethylamine / N,N-dimethyl-formamide / 48 h / 20 °C / Inert atmosphere
4: chloro-trimethyl-silane
5: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide
With
dmap; N-chloro-succinimide; chloro-trimethyl-silane; hydroxylamine hydrochloride; sodium acetate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.10.056
