C₁₉H₃₂O₂Si

Base Information

Chemical Name:C₁₉H₃₂O₂Si
CAS No.:1356926-08-3
Molecular Formula:C₁₉H₃₂O₂Si
Molecular Weight:320.547
Hs Code.:

C<sub>19</sub>H<sub>32</sub>O<sub>2</sub>Si

Synonyms:

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Chemical Property of C₁₉H₃₂O₂Si

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Technology Process of C₁₉H₃₂O₂Si

There total 10 articles about C₁₉H₃₂O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₀H₄₀O₄Si₂

: 1356926-08-3
C₁₉H₃₂O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: oxygen; palladium diacetate / dimethyl sulfoxide / 72 h / 55 °C

2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h

3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C

4: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C

5: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide

6: potassium carbonate / methanol / 6 h

With sodium tetrahydroborate; cerium(III) chloride heptahydrate; oxygen; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide; 2: Luche reduction / 6: Ohira-Bestmann reaction;
DOI:10.1016/j.tetlet.2011.12.015

Reference yield:

: 1356926-04-9
C₁₇H₃₂O₄Si

: 1356926-08-3
C₁₉H₃₂O₂Si

Guidance literature:: Multi-step reaction with 4 steps

1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C

2: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C

3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide

4: potassium carbonate / methanol / 6 h

With tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; dimethyl sulfoxide; 4: Ohira-Bestmann reaction;
DOI:10.1016/j.tetlet.2011.12.015

Reference yield:

: 1356926-06-1
C₁₈H₃₄O₃Si

: 1356926-08-3
C₁₉H₃₂O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / tetrahydrofuran; dimethyl sulfoxide

2: potassium carbonate / methanol / 6 h

With potassium carbonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dimethyl sulfoxide; 2: Ohira-Bestmann reaction;
DOI:10.1016/j.tetlet.2011.12.015