3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

Base Information

Chemical Name:3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid
CAS No.:1391999-79-3
Molecular Formula:C₂₈H₃₄N₂O₉
Molecular Weight:542.586
Hs Code.:

Synonyms:

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Chemical Property of 3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

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Technology Process of 3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

There total 9 articles about 3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391999-74-8
tert-butyl 3-(4-isopropoxy-3-nitrophenyl)acrylate

: 1391999-79-3
3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: 5%-palladium/activated carbon; hydrogen / ethanol / 14 h / Inert atmosphere

2.1: sodium hydrogencarbonate / dichloromethane; water / 0.83 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

3.2: 1 h / -78 °C / Inert atmosphere

4.1: trifluoroacetic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With 5%-palladium/activated carbon; hydrogen; potassium hexamethylsilazane; sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; toluene;
DOI:10.1039/c2ob25273b

Reference yield:

: C₁₆H₂₁ClO₅

: 1391999-79-3
3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With potassium hexamethylsilazane; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1039/c2ob25273b

Reference yield:

: 1391999-75-9
tert-butyl 3-(3-amino-4-isopropoxyphenyl)propanoate

: 1391999-79-3
3-(3-(3-allyl-3-(3-(carboxymethoxy)-5-isopropoxybenzoyl)ureido)-4-isopropoxyphenyl)propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 0.83 h / 20 °C / Inert atmosphere

2.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.25 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0.17 h / 0 °C / Inert atmosphere

With potassium hexamethylsilazane; sodium hydrogencarbonate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; toluene;
DOI:10.1039/c2ob25273b