9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

Base Information

Chemical Name:9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene
CAS No.:118210-66-5
Molecular Formula:C₃₃H₃₀S₂
Molecular Weight:490.733
Hs Code.:

9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzo<c>chrysene

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Chemical Property of 9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

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Technology Process of 9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

There total 3 articles about 9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 498-66-8
norborn-2-ene

: 118210-65-4
3-thiobenzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

: 118210-66-5
9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

Guidance literature:: In benzene; for 4h; Heating;
DOI:10.1246/bcsj.63.2540 DOI:10.1246/cl.1988.1029

Reference yield:

: 118210-62-1
3-benzoyl-3,4,5,6-tetrahydro-2-phenyl-4-phenylthio-2H-naphtho<1,2-b>thiin

: 118210-66-5
9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / sodium ethoxide / benzene; ethanol / Ambient temperature

2: 55 percent / Lawesson reagent / CS₂ / 5 h / Heating

3: 50 percent / benzene / 4 h / Heating

With Lawessons reagent; sodium ethanolate; In carbon disulfide; ethanol; benzene;
DOI:10.1246/cl.1988.1029

Reference yield:

: 118210-64-3
3-benzoyl-2-phenyl-5,6-dihydrobenzo-2H-thiochromene

: 118210-66-5
9,10,11,12,12a,12b,13,14-octahydro-6,7-diphenyl-9,12-methano-6H,8aH-5,8-dithiabenzochrysene

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Lawesson reagent / CS₂ / 5 h / Heating

2: 50 percent / benzene / 4 h / Heating

With Lawessons reagent; In carbon disulfide; benzene;
DOI:10.1246/cl.1988.1029