Technology Process of C29H31BrF3N3O5
There total 3 articles about C29H31BrF3N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 20 °C
2: pyridine; Dess-Martin periodane / dichloromethane; tert-butyl alcohol / 18 h
3: hydroxylamine hydrochloride; sodium carbonate / ethanol; water
4: chloroamine-T / methanol / 0.33 h
5: 3 h / 60 °C
With
pyridine; dimethylsulfide borane complex; hydroxylamine hydrochloride; chloroamine-T; sodium carbonate; Dess-Martin periodane;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2012.03.014
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water
2: chloroamine-T / methanol / 0.33 h
3: 3 h / 60 °C
With
hydroxylamine hydrochloride; chloroamine-T; sodium carbonate;
In
methanol; ethanol; water;
DOI:10.1016/j.bmcl.2012.03.014