2-aminobenzylphosphine

Base Information

Chemical Name:2-aminobenzylphosphine
CAS No.:54006-12-1
Molecular Formula:C₇H₁₀NP
Molecular Weight:139.137
Hs Code.:

Synonyms:

Suppliers and Price of 2-aminobenzylphosphine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-aminobenzylphosphine

Chemical Property:

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Technology Process of 2-aminobenzylphosphine

There total 4 articles about 2-aminobenzylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 104167-26-2
diethyl <(2-aminophenyl)methyl>phosphonate

: 54006-12-1
2-aminobenzylphosphine

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; for 3h; Inert atmosphere; Reflux; Schlenk technique; Glovebox;
DOI:10.1021/ic500163c

Reference yield:

: 3958-60-9
2-nitrophenylmethyl bromide

: 54006-12-1
2-aminobenzylphosphine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 12 h / Inert atmosphere; Reflux; Schlenk technique; Glovebox

2: zinc; hydrogenchloride / ethanol / 35 °C / Inert atmosphere; Schlenk technique; Glovebox

3: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux; Schlenk technique; Glovebox

With hydrogenchloride; lithium aluminium tetrahydride; zinc; In diethyl ether; ethanol; toluene;
DOI:10.1021/ic500163c

Reference yield:

: 4914-12-9
diethyl 2-nitrobenzylphosphonate

: 54006-12-1
2-aminobenzylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; hydrogenchloride / ethanol / 35 °C / Inert atmosphere; Schlenk technique; Glovebox

2: lithium aluminium tetrahydride / diethyl ether / 3 h / Inert atmosphere; Reflux; Schlenk technique; Glovebox

With hydrogenchloride; lithium aluminium tetrahydride; zinc; In diethyl ether; ethanol;
DOI:10.1021/ic500163c