C₃₀H₄₃F₃O₈

Base Information

Chemical Name:C₃₀H₄₃F₃O₈
CAS No.:1421687-76-4
Molecular Formula:C₃₀H₄₃F₃O₈
Molecular Weight:588.662
Hs Code.:

C<sub>30</sub>H<sub>43</sub>F<sub>3</sub>O<sub>8</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₄₃F₃O₈

Chemical Property:

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Technology Process of C₃₀H₄₃F₃O₈

There total 9 articles about C₃₀H₄₃F₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1421687-74-2
C₂₀H₃₆O₆

: 39637-99-5,20445-33-4
(S)-(+)-2-methoxy-2-trifluoromethyl-2-phenylacetyl chloride

: 1421687-76-4
C₃₀H₄₃F₃O₈

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1021/ja3116636

Reference yield:

: 61302-43-0
Essigsaeure-<(6S,2E)-6,7-dihydroxy-3,7-dimethyl-2-octen-1-yl>ester

: 1421687-76-4
C₃₀H₄₃F₃O₈

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / methanol / 20 °C

2.1: toluene-4-sulfonic acid / acetone / 6 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 1 h / -30 °C / Inert atmosphere

4.1: lithium bromide / tetrahydrofuran / 0.5 h / 0 °C

5.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

5.2: 20 °C

6.1: sodium hydroxide / tetrahydrofuran / 5 h / Reflux

6.2: 0 °C

7.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

7.2: 20 °C

8.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 0 °C

9.1: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

With methanesulfonamide; AD-mix β; sodium hydride; potassium carbonate; toluene-4-sulfonic acid; triethylamine; dicyclohexyl-carbodiimide; lithium bromide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; tert-butyl alcohol;
DOI:10.1021/ja3116636

Reference yield:

: 116660-94-7
(4'S,2E)-1-brom-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten

: 1421687-76-4
C₃₀H₄₃F₃O₈

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium hydroxide / tetrahydrofuran / 5 h / Reflux

2.2: 0 °C

3.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C

4.1: methanesulfonamide; AD-mix β / tert-butyl alcohol; water / 0 °C

5.1: dicyclohexyl-carbodiimide / dichloromethane / 48 h / 20 °C

With methanesulfonamide; AD-mix β; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ja3116636