C₃₅H₅₆O₃SiSn

Base Information

Chemical Name:C₃₅H₅₆O₃SiSn
CAS No.:1229041-69-3
Molecular Formula:C₃₅H₅₆O₃SiSn
Molecular Weight:671.623
Hs Code.:

C<sub>35</sub>H<sub>56</sub>O<sub>3</sub>SiSn

Synonyms:

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Chemical Property of C₃₅H₅₆O₃SiSn

Chemical Property:

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Technology Process of C₃₅H₅₆O₃SiSn

There total 1 articles about C₃₅H₅₆O₃SiSn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 688-73-3
tri-n-butyl-tin hydride

: 158478-17-2
Methyl 6-(tert-butyldiphenylsiloxy)-2-hexynoate

: 1229041-69-3
C₃₅H₅₆O₃SiSn

Guidance literature:: With copper(I) bromide dimethylsulfide complex; lithium diisopropyl amide; Inert atmosphere;
DOI:10.1021/jo300872y

Reference yield:

: 1229041-69-3
C₃₅H₅₆O₃SiSn

: tert-butyl((E)-4-((3aSR,6aSR)-2-methoxyhexahydro-2H-cyclopenta[b]furan-6a-yl)-6-phenoxyhex-4-enyloxy)-diphenylsilane

Guidance literature:: Multi-step reaction with 6 steps

1.1: diisobutylaluminium hydride / dichloromethane / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; dichloromethane / Inert atmosphere

3.1: iodine / dichloromethane / Inert atmosphere

4.1: sec.-butyllithium / hexane; tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

4.2: 0.5 h / -78 °C / Inert atmosphere

4.3: 12 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide; tetrahydrofuran / 3 h / 23 °C / Inert atmosphere

6.1: 1-((E)-6-(tert-butyldiphenylsilyloxy)-1-phenoxyhex-2-en-3-yl)-2-(2,2-dimethoxyethyl)cyclopentanol; 2,6-di-tert-butyl-4-methylpyridine / dichloromethane / 0.33 h / -78 - -20 °C / Inert atmosphere

6.2: -20 °C / Inert atmosphere

With 2,6-di-tert-butyl-4-methylpyridine; di-isopropyl azodicarboxylate; 1-((E)-6-(tert-butyldiphenylsilyloxy)-1-phenoxyhex-2-en-3-yl)-2-(2,2-dimethoxyethyl)cyclopentanol; tetrabutyl ammonium fluoride; iodine; sec.-butyllithium; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane; N,N-dimethyl-formamide; 2.1: |Mitsunobu Displacement;
DOI:10.1021/jo300872y

Reference yield:

: 1229041-69-3
C₃₅H₅₆O₃SiSn

: 1384122-51-3
tert-butyl ((E)-4-(1S,2S,4R)-4-(2-(2,2-dimethoxyethyl)-4-methyl-1-(triethylsilyloxy)cyclopentyl)-6-phenoxyhex-4-enyloxy)diphenylsilane

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran; dichloromethane / Inert atmosphere

3.1: iodine / dichloromethane / Inert atmosphere

4.1: sec.-butyllithium / tetrahydrofuran / 0.25 h / -78 °C / Inert atmosphere

4.2: 0.5 h / -78 °C / Inert atmosphere

4.3: 12 h / -78 - 23 °C / Inert atmosphere

5.1: 2,6-dimethylpyridine / dichloromethane / 0 °C / Inert atmosphere

6.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 23 °C / Inert atmosphere

7.1: pyridinium p-toluenesulfonate / dichloromethane / 5 h / 23 °C / Inert atmosphere

With 2,6-dimethylpyridine; oxalyl dichloride; di-isopropyl azodicarboxylate; iodine; sec.-butyllithium; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; 2.1: |Mitsunobu Displacement / 6.1: |Swern Oxidation;
DOI:10.1021/jo300872y