t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat

Base Information

• Chemical Name: t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat
• CAS No.: 53402-68-9
• Molecular Formula: C₂₅H₄₀O₅
• Molecular Weight: 420.59
• Mol file: 53402-68-9.mol

Synonyms:

Chemical Property of t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat

There total 5 articles about t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(benzyloxy)propanoic acid (33106-32-0,74431-49-5,100836-85-9,6625-78-1) → t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat (34867-21-5,53402-68-9,53402-69-0,53402-70-3,53402-71-4)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂SO₄

2: iBu₂AlH / hexane

3: (i) Mg, Et₂O, (ii) /BRN= 1635850/, Py

With sulfuric acid; diisobutylaluminium hydride; In hexane;

DOI:10.1246/bcsj.46.1279

Reference yield:

2-benzyloxypropionic acid methyl ester (53346-03-5) → t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat (34867-21-5,53402-68-9,53402-69-0,53402-70-3,53402-71-4)

Guidance literature:

Multi-step reaction with 2 steps

1: iBu₂AlH / hexane

2: (i) Mg, Et₂O, (ii) /BRN= 1635850/, Py

With diisobutylaluminium hydride; In hexane;

DOI:10.1246/bcsj.46.1279

Reference yield:

2-bromohexanoic acid (616-05-7) → t-Butyl 4-benzyloxy-2-n-butyl-3-isovaleryloxypentanoat (34867-21-5,53402-68-9,53402-69-0,53402-70-3,53402-71-4)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂SO₄

2: (i) Mg, Et₂O, (ii) /BRN= 1635850/, Py

With sulfuric acid;

DOI:10.1246/bcsj.46.1279

upstream raw materials:

Isovaleric anhydride

tert-Butyl 2R-Bromo-5-methylpentanoate

2-(benzyloxy)propanal

2-bromohexanoic acid