5,6-didehydro-10-methylbenzocyclooctene DIB adduct

Base Information

Chemical Name:5,6-didehydro-10-methylbenzocyclooctene DIB adduct
CAS No.:74611-02-2
Molecular Formula:C₃₃H₂₄O
Molecular Weight:436.553
Hs Code.:

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Chemical Property of 5,6-didehydro-10-methylbenzocyclooctene DIB adduct

Chemical Property:

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Technology Process of 5,6-didehydro-10-methylbenzocyclooctene DIB adduct

There total 3 articles about 5,6-didehydro-10-methylbenzocyclooctene DIB adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 7111-67-3
1,3-diphenyl-1,3-dihydroisobenzofuran

: 74610-98-3
5-bromo-10-methylbenzocyclooctene

: 74611-02-2
5,6-didehydro-10-methylbenzocyclooctene DIB adduct

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 48h;
DOI:10.1016/S0040-4020(01)88542-2

Reference yield: 17.0%

: 5471-63-6
1,3-diphenylisobenzofuran

: 74610-98-3
5-bromo-10-methylbenzocyclooctene

: 74611-02-2
5,6-didehydro-10-methylbenzocyclooctene DIB adduct

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; Mechanism;
DOI:10.1016/S0040-4039(00)77758-6

Reference yield:

: 17557-54-9
5,10-dibromobenzocyclooctene

: 74611-02-2
5,6-didehydro-10-methylbenzocyclooctene DIB adduct

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / diethyl ether / 1 h / Ambient temperature

2: 17 percent / KOtBu / tetrahydrofuran / 48 h

With potassium tert-butylate; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)88542-2