C₁₄H₁₉O₁₃P₃

Base Information

Chemical Name:C₁₄H₁₉O₁₃P₃
CAS No.:1428632-10-3
Molecular Formula:C₁₄H₁₉O₁₃P₃
Molecular Weight:488.218
Hs Code.:

C<sub>14</sub>H<sub>19</sub>O<sub>13</sub>P<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₉O₁₃P₃

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Technology Process of C₁₄H₁₉O₁₃P₃

There total 3 articles about C₁₄H₁₉O₁₃P₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1446517-59-4
C₂₀H₃₃O₁₃P₃Si

: 1428632-10-3
C₁₄H₁₉O₁₃P₃

Guidance literature:: With ammonium hydroxide; at 20 ℃; for 1h;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-86-0
C₁₂H₁₅IO₄

: 1428632-10-3
C₁₄H₁₉O₁₃P₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: trimethyl phosphite; trichlorophosphate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / -15 - 10 °C / Inert atmosphere

1.2: 0.5 h / -10 - 0 °C

2.1: trisodium tris(3-sulfophenyl)phosphine; copper(l) iodide; palladium diacetate; triethylamine / water; acetonitrile / 0.5 h / 20 - 55 °C / Inert atmosphere

3.1: ammonium hydroxide / 1 h / 20 °C

With trimethyl phosphite; ammonium hydroxide; copper(l) iodide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene; triethylamine; trichlorophosphate; In water; acetonitrile; 2.1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja312148q

Reference yield:

: 1428631-89-3
C₁₂H₁₈IO₁₃P₃

: 1428632-10-3
C₁₄H₁₉O₁₃P₃

Guidance literature:: Multi-step reaction with 2 steps

1: trisodium tris(3-sulfophenyl)phosphine; copper(l) iodide; palladium diacetate; triethylamine / water; acetonitrile / 0.5 h / 20 - 55 °C / Inert atmosphere

2: ammonium hydroxide / 1 h / 20 °C

With ammonium hydroxide; copper(l) iodide; trisodium tris(3-sulfophenyl)phosphine; palladium diacetate; triethylamine; In water; acetonitrile; 1: |Sonogashira Cross-Coupling;
DOI:10.1021/ja312148q