Technology Process of trans-1-(benzylamino)-4-chlorocycloheptane HCl
There total 6 articles about trans-1-(benzylamino)-4-chlorocycloheptane HCl which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / Me4NIO4 / CHCl3; dimethylformamide
2: 92 percent / Al/Hg / tetrahydrofuran; H2O
3: 99 percent / H2 / Pd/C / methanol
4: 99 percent / LiAlH4 / diethyl ether
5: SOCl2 / CHCl3
With
aluminum amalgam; lithium aluminium tetrahydride; thionyl chloride; tetramethylammonium metaperiodate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81095-9
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 99 percent / Me4NIO4 / CHCl3; dimethylformamide
2: 92 percent / Al/Hg / tetrahydrofuran; H2O
3: 99 percent / H2 / Pd/C / methanol
4: 99 percent / LiAlH4 / diethyl ether
5: SOCl2 / CHCl3
With
aluminum amalgam; lithium aluminium tetrahydride; thionyl chloride; tetramethylammonium metaperiodate; hydrogen;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; diethyl ether; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)81095-9
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / H2 / Pd/C / methanol
2: 99 percent / LiAlH4 / diethyl ether
3: SOCl2 / CHCl3
With
lithium aluminium tetrahydride; thionyl chloride; hydrogen;
palladium on activated charcoal;
In
methanol; diethyl ether; chloroform;
DOI:10.1016/S0040-4039(01)81095-9