Technology Process of ethyl(2-ethoxycarbonylmethoxy-4-methoxyphenyl)acetate
There total 10 articles about ethyl(2-ethoxycarbonylmethoxy-4-methoxyphenyl)acetate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent / diethyl ether / 0 °C
2: 92 percent / potassium carbonate, potassium iodide / 4 h / Heating
3: 1.) potassium metabisulfite / 1.) 50 deg C, water 2.) water, ether, 5 deg C, 6 h
4: stannous chloride dihydrate, cc. hydrogen chloride, acetic acid, hydrogen iodide / 3 h / Heating
5: 77 percent / cc. sulfuric acid / 12 h / Heating
With
hydrogenchloride; potassium disulphite; sulfuric acid; hydrogen iodide; potassium carbonate; acetic acid; potassium iodide; tin(ll) chloride;
In
diethyl ether;
DOI:10.1002/bscb.19800890607
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 92 percent / potassium carbonate, potassium iodide / 4 h / Heating
2: 1.) potassium metabisulfite / 1.) 50 deg C, water 2.) water, ether, 5 deg C, 6 h
3: stannous chloride dihydrate, cc. hydrogen chloride, acetic acid, hydrogen iodide / 3 h / Heating
4: 77 percent / cc. sulfuric acid / 12 h / Heating
With
hydrogenchloride; potassium disulphite; sulfuric acid; hydrogen iodide; potassium carbonate; acetic acid; potassium iodide; tin(ll) chloride;
DOI:10.1002/bscb.19800890607
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) morpholine, sulfur 2.) 10 percent aq. sodium hydroxide / 1.) 160 deg C, 4 h 2.) reflux, 4 h
2: 80 percent / sulfuric acid / Heating
3: potassium carbonate / 6 h / Heating
With
morpholine; sodium hydroxide; sulfuric acid; potassium carbonate; sulfur;
DOI:10.1002/bscb.19800890607
