4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine

Base Information

Chemical Name:4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine
CAS No.:1267990-93-1
Molecular Formula:C₂₈H₂₆ClN₃O₅S
Molecular Weight:552.051
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine

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Technology Process of 4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine

There total 2 articles about 4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1267990-93-1
4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Cooling with ice; Inert atmosphere;

In dichloromethane; at 20 ℃;

Reference yield:

: 1267986-38-8
4-Chlorodeacetylcolchicine

: 1267990-93-1
4-chloro-N-[(3-cyanophenyl)thiocarbamoyl]deacetyl colchicine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

2: dichloromethane / 0 - 20 °C / Inert atmosphere

With triethylamine; In dichloromethane;
DOI:10.1039/c3md00287j