(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

Base Information

Chemical Name:(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506
CAS No.:128685-14-3
Molecular Formula:C₈₅H₁₄₅NO₁₅Si₃
Molecular Weight:1505.34
Hs Code.:

(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

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Chemical Property of (9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

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Technology Process of (9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

There total 1 articles about (9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₈₅H₁₄₇NO₁₅Si₃

: 128685-14-3,128777-62-8
(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 1.25h; Yield given; Ambient temperature;
DOI:10.1021/ja00170a024

Reference yield:

: 128685-14-3,128777-62-8
(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9-<(2,4-dimethoxybenzyl)oxy>-22-<(4-methoxybenzyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

: 128685-16-5,128777-66-2
(9RS,22S)-14-<(tert-butyldimethylsilyl)oxy>-9,22-tetrahydro-24,32-bis<(triisopropylsilyl)oxy>-FK506

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; tert-butyl alcohol; for 3.25h; Yield given;
DOI:10.1021/ja00170a024