Technology Process of C23H18O5S
There total 5 articles about C23H18O5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 16 h / 65 °C / Inert atmosphere
2: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
3: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere
4: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; stabilized 2-iodoxybenzoic acid; Au(OAc)3; tetrabutyl ammonium fluoride; triethylamine;
In
dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
1: Sonogashira coupling;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 3 steps
1: Au(OAc)3 / 1,2-dichloro-ethane / 20 °C / Inert atmosphere
2: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere
3: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
stabilized 2-iodoxybenzoic acid; Au(OAc)3; tetrabutyl ammonium fluoride;
In
dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/co300002x
- Guidance literature:
-
Multi-step reaction with 2 steps
1: stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride / 20 °C / Inert atmosphere
2: polystyrene supported 4-dimethylaminopyridine / dichloromethane / Inert atmosphere
With
stabilized 2-iodoxybenzoic acid; tetrabutyl ammonium fluoride;
In
dichloromethane;
DOI:10.1021/co300002x
